Insoluble in the normal reagents.
1348
The unknown is not acidic nor basic.
Peak near 9ppm is exchangeable. Solvent is deuterochloroform.
ǾǼ
Ⱦyn!   ]az
N!>%u" #
L
#
Assignments may be 5 Ar (Ph ?), isolated methylene and methyl, 1 exchangeable.
#
dummy ms
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Only nitrogen was found.
264048
Halogens and sulfur are not present in this compound.
No residue was left after burning with a smoky flame.
#
The compound is probably aromatic and completely organic.
83-85 degrees.
#
A low melting solid.
Nujol mull
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ަob`[`kqXCP^||h\RPafaec|ztjZWastozumszkktwlcSDAECA>;=CO?51...02;Eb|ocNA:731/...----0473-,++++-0561//3401..2750,*)(()),?D/+*((-382-+)))'(**)('()+.4V}rbQNRVWZ]YZd72.+(''1<,(&'""""!""&++1)%#&,PI,4WM)%#"$&%"!!   $$(+-.  
#
The compound is a monosubstituted amide with a monosubstituted benzene ring.
Too high - decomposition occurred.
#
Typical behaviour for a solid.
Optically inactive.
#
The molecule is not chiral.
Not usually measured for a solid.
#
Best to make this measurement on a liquid.
Not usually measured for a solid.
#
Measure this for a liquid.
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dummy cmr
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A yellow precipitate formed.
#
The unknown contains an aldehyde or ketone group.
No positive result.
3344454651
The unknown is not an alcohol, phenol or acid.
No positive result was obtained.
#
This compound is not a primary or secondary amine.
No colour change could be seen.
#
The unknown is not an aldehyde.
#
#
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No reaction could be seen.
14
The unknown is not an ester.
No apparent reaction took place.
#
Nitro groups are absent from the compound.
#
#
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A yellow coloured precipitate formed.
#
A methylketone group is present.
No positive result was seen.
#
The compound is not an aldehyde (nor a monosaccharide).
No silver mirror formed.
#
No aldehyde group is present in this unknown.
No positive result.
3344454651
The compound is not an alcohol, phenol or a primary or secondary amine.
A red colour formed.
#
This result shows that the compound is an amide or cyanide (nitrile).
No reaction was noticed.
#
The compound is not unsaturated nor is it easily oxidised.
#
#
#
No colour change was observed.
23
The compound is not a sugar.
No observable change.
#
No nitro groups are present.
No reaction was seen.
#
The unknown is not a phenol nor is it unsaturated.
No positive result.
#
The compound is not an ether.
A red colour developed.
#
The unknown is either a phenol or an enol.
No reaction was observed.
#
The compound is not a primary amine.
#
#
#
No reaction.
#
This result indicates that the compound is not a primary or secondary amine.
No apparent change could be seen.
#
The unknown is not an amino acid.
No positive result.
#
No foul smell equals no primary amine.
#
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A vigorous reaction giving a solution took place.
#
Typical of N- and/or O-containing compounds.
#
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No change could be seen.
#
The unknown is not a primary amine.
No positive result could be observed.
#
The unknown is not an aldehyde.
#
#
#
No reaction occurred.
#
The compound is not unsaturated. It is also not a phenol.
The compound reacted with aqueous base to give an insoluble liquid product.
#
The hydrolysis product is a water insoluble, nonvolatile liquid:- eg an amine.
No positive result.
3344454651
The unknown is not an alcohol, phenol or amine (prim. or sec.).
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colourless solid
010507
3153

2
įc^
yPqq[
solid amide
3
acetoacetanilide
ethylphenylacetanilide
4-n-propylacetanilide
